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Preparation of 5-Substituted 1H-Tetrazoles catalyzed by scandium triflate in water
Resource type
Authors/contributors
- Coca, Adiel (Author)
- Turek, Evan (Author)
- Feinn, Liana (Author)
Title
Preparation of 5-Substituted 1H-Tetrazoles catalyzed by scandium triflate in water
Abstract
Several 5-substituted 1H-tetrazoles were prepared in water or isopropanol/water mixtures using microwave heating. Good yields were obtained for the [2 + 3] cycloaddition of sodium azide with aryl nitriles, aliphatic nitriles, and vinyl nitriles when catalyzed by scandium triflate. The reactions were typically heated for 1 h at 160 °C in a 3:1 isopropanol/water mixture to obtain the best yields. © 2015 Taylor & Francis Group, LLC.
Publication
Synthetic Communications
Date
2015
Volume
45
Issue
2
Pages
218-225
Journal Abbr
Synth. Commun.
Citation Key
pop00027
ISSN
00397911 (ISSN)
Language
English
Extra
10 citations (Crossref) [2023-10-31]
Citation Key Alias: lens.org/083-255-404-167-567
tex.type: [object Object]
Citation
Coca, A., Turek, E., & Feinn, L. (2015). Preparation of 5-Substituted 1H-Tetrazoles catalyzed by scandium triflate in water. Synthetic Communications, 45(2), 218–225. https://doi.org/10.1080/00397911.2014.957775
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